01-073-6463 Na1.554 K.296 Mg2 Si30.15 Al5.85 O72 ( H2 O )18 Al5.85 H36 K0.296 Mg2 Na1.554 O90 Si30.15 Sodium Potassium Magnesium Silicon Aluminum Oxide Hydrate Ferrierite-Mg Sodium potassium magnesium tecto-alumosilicate hydrate Orthorhombic 2.111 1.98 Ambient Primary 19.1560(50) 14.1270(30) 7.4890(30) 1.00 2026.65 2026.65 0.391 1.356 0.530 2026.65 1013.32 14.127 19.156 7.489 90.00 90.00 90.00 0.530 0.737 0.391 7.489 12.476 12.476 68.97 72.53 72.53 1.00 F(30) = 212.5(0.0042, 34) Immm (71) 2576.76 Blank (B) 1.97 1.5406 CuKá1 Calculated Calculated 71 Space Group Immm (71) 0.107 oI165.85 oI129.85 11/19/2008 01/19/2011 Al6.13 H1.41 K0.45 Mg1.89 Na1.39 O55.88 Si32.86 Al3.53 H21.71 K0.18 Mg1.21 Na0.94 O54.27 Si18.18 ICSD Pattern, Primary Pattern, Inorganic, Mineral Related (Mineral , Natural) Primary Reference Calculated from ICSD using POWD-12++. Structure "The crystal structure of the zeolite ferrierite". Vaughan, P.A. Acta Crystallogr. 21, 983 (1966). Analysis: H36 Al5.85 K0.296 Mg2 Na1.554 O90 Si30.15. Formula from original source: Na1.554 K0.296 Mg2 (Si30.15 Al5.85 O72) (H2 O)18. ICSD Collection Code: 35082. Calculated Pattern Original Remarks: Mean T-O: 1.613, 1.626, 1.599, 1.596; mean T-O-T: 158 degree (at O5 linear). AE: (Si, Al): 4t O4; O1-8: 2n (Si, Al)2; Mg: (H2 O)6; O9-11: Mg H2. Zeolite-FER. Minor Warning: 7%<R factor<12% (for single crystal). Significant Warning: Density calculated using chemical formula and reported structure differ by 6.1611%. Reported displacement parameters on non H atoms are outside the range 0.001<U<0.1. Ueq=0.012 used in the calculation. Wyckoff Sequence: o3 n5 m2 k i g f e2 c(IMMM). Unit Cell Data Source: Single Crystal. Centrosymmetric 1.54056 PDF Card - 01-073-6463_Ferrierite-Mg_169%.jpg 7.7694 11.369600 492 1 1 0 9.2256 9.578000 999 2 0 0 12.5212 7.063500 101 0 2 0 12.6809 6.974920 147 1 0 1 13.3703 6.616750 83 0 1 1 15.2146 5.818570 237 3 1 0 15.5749 5.684800 28 2 2 0 16.2683 5.444010 2 2 1 1 17.8572 4.963030 51 1 2 1 18.2430 4.858930 5 3 0 1 18.5117 4.789000 23 4 0 0 19.3950 4.572860 16 1 3 0 22.1875 4.003230 272 3 2 1 22.2822 3.986420 115 0 3 1 22.4107 3.963850 216 4 2 0 22.9046 3.879490 150 4 1 1 23.4538 3.789870 170 3 3 0 23.7421 3.744500 38 0 0 2 24.0474 3.697640 70 5 1 0 25.0163 3.556580 175 1 1 2 25.1951 3.531750 295 0 4 0 25.5204 3.487460 368 2 0 2 26.1041 3.410790 63 5 0 1 26.8834 3.313660 75m 0 2 2 26.8834 3.313660 m 2 4 0 27.9224 3.192670 12 6 0 0 28.3194 3.148810 146m 3 1 2 28.3194 3.148810 m 1 4 1 28.5204 3.127080 21 2 2 2 29.0482 3.071450 93m 5 2 1 29.0482 3.071450 m 4 3 1 30.0442 2.971860 75 5 3 0 30.2739 2.949830 25 4 0 2 30.8381 2.897130 53 1 3 2 31.0766 2.875440 9 6 1 1 31.2843 2.856820 2 3 4 1 31.4471 2.842400 8 4 4 0 31.9927 2.795160 3 1 5 0 32.8767 2.722000 37 4 2 2 33.3220 2.686630 8 7 1 0 33.8817 2.643520 42 0 5 1 34.0473 2.631040 7 5 1 2 34.6899 2.583760 28 3 5 0 34.8921 2.569250 22m 7 0 1 34.8921 2.569250 m 0 4 2 35.1890 2.548250 1 2 5 1 36.0104 2.491980 8 6 3 1 36.1675 2.481520 12 2 4 2 36.5218 2.458250 1m 0 1 3 36.5218 2.458250 m 5 4 1 36.9702 2.429460 29 6 0 2 37.1934 2.415390 6 7 2 1 37.5300 2.394500 1 8 0 0 37.9984 2.366050 33m 7 3 0 37.9984 2.366050 m 6 4 0 38.5047 2.336100 5 1 2 3 38.6963 2.324970 3m 5 3 2 38.6963 2.324970 m 3 0 3 38.8812 2.314340 21 4 5 1 39.1801 2.297370 2 6 2 2 39.3753 2.286430 2 2 6 0 39.7816 2.264010 12m 8 2 0 39.7816 2.264010 m 4 4 2 40.0102 2.251600 8 8 1 1 40.2278 2.239920 6 1 5 2 40.3988 2.230830 3 1 6 1 40.8269 2.208420 1m 3 2 3 40.8269 2.208420 m 0 3 3 41.2457 2.186960 10m 4 1 3 41.2457 2.186960 m 7 1 2 42.0017 2.149330 16 2 3 3 42.4716 2.126630 3 3 5 2 42.6353 2.118840 9 3 6 1 42.7602 2.112940 33 4 6 0 42.9361 2.104690 8 9 1 0 43.2200 2.091520 1 5 0 3 43.5105 2.078230 1 7 4 1 44.2008 2.047360 18 9 0 1 44.4573 2.036140 9 6 5 1 44.6670 2.027070 4 1 4 3 44.8950 2.017300 6 8 0 2 45.1749 2.005450 43m 5 2 3 45.1749 2.005450 m 4 3 3 45.2664 2.001610 30m 6 4 2 45.2664 2.001610 m 7 3 2 45.4678 1.993210 4 0 6 2 45.7415 1.981920 16 8 4 0 46.1227 1.966420 18m 7 5 0 46.1227 1.966420 m 9 2 1 46.5685 1.948630 26m 0 7 1 46.5685 1.948630 m 6 1 3 46.8002 1.939520 26m 9 3 0 46.8002 1.939520 m 5 6 1 47.1922 1.924320 24 3 7 0 47.4202 1.915600 5 10 0 0 47.5807 1.909510 2 2 7 1 47.9697 1.894930 2 6 6 0 48.5881 1.872250 68m 0 5 3 48.5881 1.872250 m 0 0 4 49.2857 1.847370 6m 1 1 4 49.2857 1.847370 m 10 2 0 49.6097 1.836060 7m 2 5 3 49.6097 1.836060 m 9 1 2 50.2347 1.814670 10 6 3 3 50.5248 1.804930 1 4 7 1 50.6844 1.799620 1 5 4 3 51.1121 1.785560 54m 5 7 0 51.1121 1.785560 m 7 2 3 51.4480 1.774690 17 8 5 1 51.6272 1.768950 16m 9 4 1 51.6272 1.768950 m 1 7 2 52.1740 1.751690 8 8 4 2 52.5363 1.740460 2m 7 5 2 52.5363 1.740460 m 4 5 3 52.6617 1.736610 3m 2 8 0 52.6617 1.736610 m 7 6 1 52.9907 1.726600 4m 11 1 0 52.9907 1.726600 m 10 3 1 53.1364 1.722210 6 9 3 2 53.3687 1.715260 2 8 1 3 53.4939 1.711540 5m 1 8 1 53.4939 1.711540 m 3 7 2 53.6808 1.706020 1m 1 6 3 53.6808 1.706020 m 10 0 2 53.8849 1.700040 1 9 5 0 54.2048 1.690760 1m 6 6 2 54.2048 1.690760 m 4 2 4 54.6304 1.678590 6m 8 6 0 54.6304 1.678590 m 3 3 4 54.9229 1.670340 9 5 1 4 55.3061 1.659670 15 3 8 1 55.4090 1.656830 13m 10 2 2 55.4090 1.656830 m 4 8 0 55.5051 1.654190 14m 3 6 3 55.5051 1.654190 m 0 4 4 55.6836 1.649310 5 11 2 1 56.2762 1.633340 10m 7 4 3 56.2762 1.633340 m 11 3 0 56.3995 1.630060 3 2 4 4 56.6202 1.624230 12m 7 7 0 56.6202 1.624230 m 8 3 3 56.7952 1.619640 11 9 0 3 57.0091 1.614070 10m 6 0 4 57.0091 1.614070 m 6 5 3 57.7018 1.596330 13m 0 8 2 57.7018 1.596330 m 12 0 0 58.1897 1.584100 5 5 3 4 58.7933 1.569270 4m 11 1 2 58.7933 1.569270 m 5 8 1 59.0246 1.563670 13m 4 4 4 59.0246 1.563670 m 5 6 3 59.2997 1.557070 4m 12 2 0 59.2997 1.557070 m 1 5 4 59.6496 1.548770 11m 2 7 3 59.6496 1.548770 m 9 5 2 59.7989 1.545260 5m 6 8 0 59.7989 1.545260 m 9 6 1 60.1844 1.536280 9m 0 9 1 60.1844 1.536280 m 7 1 4 60.5008 1.529000 2 11 4 1 60.7074 1.524290 4 3 9 0 61.0716 1.516070 3m 4 8 2 61.0716 1.516070 m 3 5 4 61.2986 1.511000 2m 8 7 1 61.2986 1.511000 m 10 1 3 61.9296 1.497110 23 11 3 2 62.2538 1.490090 4m 7 7 2 62.2538 1.490090 m 0 1 5 62.4476 1.485930 1 10 6 0 62.6352 1.481930 10m 11 5 0 62.6352 1.481930 m 12 3 1 63.0961 1.472210 16m 9 4 3 63.0961 1.472210 m 2 1 5 63.2888 1.468190 14m 7 3 4 63.2888 1.468190 m 12 0 2 63.4678 1.464480 17m 9 7 0 63.4678 1.464480 m 4 9 1 63.7723 1.458220 1 3 0 5 63.9478 1.454640 3m 7 8 1 63.9478 1.454640 m 12 4 0 64.0834 1.451890 5m 5 9 0 64.0834 1.451890 m 7 6 3 64.3623 1.446270 6m 10 3 3 64.3623 1.446270 m 13 0 1 64.4867 1.443780 6m 1 9 2 64.4867 1.443780 m 8 2 4 64.7992 1.437570 11m 1 8 3 64.7992 1.437570 m 12 2 2 65.2661 1.428410 57m 6 8 2 65.2661 1.428410 m 3 2 5 65.6388 1.421200 17m 4 1 5 65.6388 1.421200 m 8 8 0 66.0840 1.412700 17m 0 10 0 66.0840 1.412700 m 2 3 5 66.3091 1.408450 4 6 7 3 66.4268 1.406240 5m 13 3 0 66.4268 1.406240 m 3 8 3 66.7652 1.399930 8m 11 2 3 66.7652 1.399930 m 9 1 4